Synthesis conditions of ZBLAN glass for mid-infrared optical components

Authors

  • Jarosław Cimek
  • Xavier Forestier
  • Ryszard Stepien
  • Mariusz Klimczak
  • Ryszard Buczynski University of Warsaw

DOI:

https://doi.org/10.4302/plp.v10i1.804

Abstract

We report on successful synthesis of ZBLAN glass. Different purity of zirconium tetrafluoride used for synthesis and fluorinating agents were analyzed to obtain high optical quality glass. Among fluorinating agents we used ammonium bifluoride, xenon difluoride and sulfur hexafluoride. The best results in form of synthetized glasses have transmission window extending from 0.2 to 8.0 um, which allows to fabricate fibers for mid-infrared applications.

Full Text: PDF

References
  1. R. Stępień, J. Cimek, D. Pysz, I. Kujawa, M. Klimczak, and R. Buczyński, Soft glasses for photonic crystal fibers and microstructured optical components, Opt. Eng. 53, 071815 (2014). CrossRef
  2. D. Pysz, I. Kujawa, R. Stępień, M. Klimczak, A. Filipkowski, M. Franczyk, L. Kociszewski, J. Buźniak, K. Haraśny, R. Buczyński, Stack and draw fabrication of soft glass microstructured fiber optics, Bull. Pol. Acad. Sci.-Tech. Sci., 62(4), 667-683 (2014). CrossRef
  3. R. Kasztelanic, I. Kujawa, R. Stępień, K. Haraśny, D. Pysz and R. Buczyński, Molding of soft glass refraction mini lens with hot embossing process for broadband infrared transmission systems, Infrared Phys. Technol. 61, 299-305 (2013). CrossRef
  4. Moynihan C.T. (1987) Crystallization Behavior of Fluorozirconate Glasses. In: Almeida R.M. (eds) Halide Glasses for Infrared Fiberoptics. NATO ASI Series (Series E: Applied Sciences), 123, Springer, Dordrecht. CrossRef
  5. M. R. Majewski, R. I. Woodward, S. D. Jackson, Dysprosium-doped ZBLAN fiber laser tunable from 2.8?m to 3.4?m, pumped at 1.7?m, Opt. Lett. 43, 971-974 (2018). CrossRef
  6. G Bharathan, R. I. Woodward, M. Ams, D. D. Hudson, S. D. Jackson, A. Fuerbach, Direct inscription of Bragg gratings into coated fluoride fibers for widely tunable and robust mid-infrared lasers, Opt. Express 25, 30013-30019 (2017). CrossRef
  7. Y. Shen, Y. Wang, H. Chen, K. Luan, M. Tao, J. Si, Wavelength-tunable passively mode-locked mid-infrared Er3+-doped ZBLAN fiber laser, Sci. Rep. 7, 14913 (2017). CrossRef
  8. J. Méndez-Ramos, P. Acosta-Mora, J. C. Ruiz-Morales, T. Hernández, M. E. Borges, P. Esparza, Heavy rare-earth-doped ZBLAN glasses for UV?blue up-conversion and white light generation, J. Lumin. 143, 479-483 (2013). CrossRef
  9. X. Jiang, N. Y. Joly, M. A. Finger, F. Babic, G. K. L. Wong, J. C. Travers, P. St. J. Russell, Deep-ultraviolet to mid-infrared supercontinuum generated in solid-core ZBLAN photonic crystal fibre, Nat. Photonics 9, 133?139 (2015). CrossRef
  10. X. Jiang, N. Y. Joly, M. A. Finger, F. Babic, M. Pang, R. Sopalla, M. H. Frosz, S. Poulain, M. Poulain, V. Cardin, J. C. Travers, P. St. J. Russell, Supercontinuum generation in ZBLAN glass photonic crystal fiber with six nanobore cores, Opt. Lett. 41, 4245-4248 (2016). CrossRef
  11. A. Medjouri, E. B. Meraghni, H. Hathroubi, D. Abed, L. M. Simohamed, O. Ziane, Design of ZBLAN photonic crystal fiber with nearly zero ultra-flattened chromatic dispersion for supercontinuum generation, Optik 135, 417?425 (2017). CrossRef
  12. D. C. Tee, N. Tamchek, C. H. Raymond Ooi, Numerical Modeling of the Fundamental Characteristics of ZBLAN Photonic Crystal Fiber for Communication in 2?3 ?m Midinfrared Region, IEEE Photon. J. 8, 4500713 (2016) . CrossRef
  13. Y. Dai, K. Takahashi, I. Yamaguchi, Thermal oxidation of fluorozirconate glass and fibres, J. Mater. Sci. Lett. 12, 1648?1651 (1993). CrossRef
  14. P. Hlubina, White-light spectral interferometry with the uncompensated Michelson interferometer and the group refractive index dispersion in fused silica, Opt. Commun. 193, 1-7 (2001). CrossRef
  15. F. Gan, Optical properties of fluoride glasses: a review, J. Non Cryst. Sol. 184, 9-20 (1995). CrossRef
  16. A. Filipkowski, B. Piechal, D. Pysz, R. Stepien, A. Waddie, M. R. Taghizadeh, and R. Buczynski, Nanostructured gradient index micro axicons made by a modified stack and draw method, Opt. Lett. 40, 5200-5203 (2015). CrossRef
  17. R. Kasztelanic, A. Filipkowski, D. Pysz, R. Stepień, A. J. Waddie, M. R. Taghizadeh, and R. Buczynski, High resolution Shack-Hartmann sensor based on array of nanostructured GRIN lenses, Opt. Express 25, 1680-1691 (2017). CrossRef

Downloads

Published

2018-03-31

How to Cite

[1]
J. Cimek, X. Forestier, R. Stepien, M. Klimczak, and R. Buczynski, “Synthesis conditions of ZBLAN glass for mid-infrared optical components”, Photonics Lett. Pol., vol. 10, no. 1, pp. 8–10, Mar. 2018.

Issue

Section

Articles